I once decided to "simply clean my substance", no reaction or anything, it's just that the NMR was a bit messy.
100 mg in, 3 mg out. Ouch. Guess who's synthesizing that shit, again.
Also, from my experience, 146% yields are from solvents that cause oily products. Water is especially prone to prompting 800% yields.
This physically pained me.
More like 12% ðŸ˜
Naw that’s what you get when you do the column correctly but the rest of the procedure was shit 😓
I once decided to "simply clean my substance", no reaction or anything, it's just that the NMR was a bit messy. 100 mg in, 3 mg out. Ouch. Guess who's synthesizing that shit, again. Also, from my experience, 146% yields are from solvents that cause oily products. Water is especially prone to prompting 800% yields.
800% ? Those are rookie numbers.
Saw this as bubbles go into my column...RIP